| 引用本文: | 黄汉昌,姜瑞瑞,张明贤.β-榄香烯的分析检测方法及制备技术研究进展[J].中国现代应用药学,2011,28(2):116-120. |
| HUANG Hanchang,JIANG Ruirui,ZHANG Mingxian.The Progress on Analytical Methods and Isolated Techniques on the Development of β-Elemene[J].Chin J Mod Appl Pharm(中国现代应用药学),2011,28(2):116-120. |
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| 摘要: |
| 目的 介绍β-榄香烯的分析检测方法及制备技术研究进展。方法 本文对榄香烯的双键异构及β-榄香烯的光学异构体分子结构、分析检测方法及制备技术进行了综述；进一步评述从天然植物中提取及分离β-榄香烯的方法及技术的优缺点。结果与结论 气相或液相色谱结合核磁、质谱等光谱技术能较好地检测β-榄香烯成分及含量；众多植物挥发油富含β-榄香烯，采用真空精馏及柱层析联用技术能获得高纯度的β-榄香烯。 |
| 关键词: β-榄香烯 提取 分离 分析 |
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| 基金项目:北京市教育委员会科技计划项目(KM201011417002) |
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| The Progress on Analytical Methods and Isolated Techniques on the Development of β-Elemene |
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HUANG Hanchang, JIANG Ruirui, ZHANG Mingxian
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Beijing Union University, a.Beijing Key Laboratory of Bioactive Substances and Functional Foods, b.College of Arts and Science, c.College of Biochemical Engineering, Beijing 100191, China
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| Abstract: |
| OBJECTIVE To review the progress of β-elemene on the analytical methods and isolated techniques. METHODS This article provides an overview about the structures of elemene’s cis-trans isomers and optical isomers of β-elemene, the analytical methods and isolated techniques of β-elemene, and further comment of advantages and disadvantages on the extraction and isolation of β-elemene from natural products. RESULTS and CONCLUSION β-elemene will be well detected by gas or liquid chromatography plus spectrum techniques, like nuclear magnetic resonance (NMR) and mass spectrum (MS). β-elemene is contained on a host of essential oils and will be well isolated by the combined techniques of vacuum distillation and column chromatography. |
| Key words: β-elemene extraction separation analysis |
