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引用本文:韩娜,赵建邦,宋平顺.莱菔子脂溶性成分的GC-MS分析[J].中国现代应用药学,2011,28(1):74-76.
HAN Na,ZHAO Jianbang,SONG Pingshun.Analysis of Fat-soluble Components in Raphani Semen by GC-MS[J].Chin J Mod Appl Pharm(中国现代应用药学),2011,28(1):74-76.
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莱菔子脂溶性成分的GC-MS分析
韩娜1, 赵建邦1, 宋平顺2
1.甘肃农业大学农学院,兰州 730000;2.甘肃省药品检验所,兰州 730000
摘要:
目的 探讨莱菔子脂溶性成分的组成及相对含量。方法 采用超声法提取莱菔子油,KOH甲醇溶液甲酯化,通过气相色谱-质谱联用技术分析莱菔子中脂溶性成分。结果 从莱菔子油中共分离鉴定出27中脂溶性成分,15种脂肪酸成分,其相对含量占总成分的50.47%;另有12种成分未见文献报道。结论 本方法简便、快速、分离效果好,适用于莱菔子脂溶性成分的分析研究。
关键词:  莱菔子  脂溶性成分  气相色谱-质谱联用技术
DOI:
分类号:
基金项目:甘肃省科学技术攻关计划项目(GS035-A43-048-03)
Analysis of Fat-soluble Components in Raphani Semen by GC-MS
HAN Na1, ZHAO Jianbang1, SONG Pingshun2
1.Gansu Agriculture University, Lanzhou 730000, China;2.Gansu Institute for Drug Control, Lanzhou 730000, China
Abstract:
OBJECTIVE To discuss the constituents and reletive contents on fat-soluble components in Raphani Semen. METHODS The oil from Raphani Semen was extracted by ultrasonic technology, then esterified with KOH-CH3OH and analysised by GC-MS. RESULTS There were 27 fat-soluble components identified, inclouding 15 fatty acids components which were accounting for 50.47% of the total components, 12 components had not been reported in documents. CONCLUSION The method is simple, efficient and could be used for the study of the fat-soluble components in Raphani Semen.
Key words:  Raphani Semen  fat-soluble components  GC-MS
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