| 引用本文: | 张士英1,2;卢冠忠1.从邻苯二甲酰亚胺合成依托酸酐[J].中国现代应用药学,2007,(6):473-474. |
| ZHANG Shi-ying1,2,LU Guan-zhong2.Synthesis of Isatoic Anhydride from Phthalimide[J].Chin J Mod Appl Pharm(中国现代应用药学),2007,(6):473-474. |
|
|
| 摘要: |
| 目的合成标题化合物,并进行工艺改进。方法以邻苯二甲酰亚胺为原料经次氯酸钠氧化合成目标化合物。结果收率达90%以上,产物经红外和核磁共振谱确证。结论改进的路线原子经济、环境友好,易操作。 |
| 关键词: 依托酸酐 邻苯二甲酰亚胺 合成 |
| DOI： |
| 分类号: |
| 基金项目: |
|
| Synthesis of Isatoic Anhydride from Phthalimide |
|
ZHANG Shi-ying1,2,LU Guan-zhong2
|
| Abstract: |
| OBJECTIVE To synthesize the title compound and improve the process.METHODS The title compound was synthesized from phthalimide by oxidation with sodium hypochlorite.RESULTS The yield was up to 90%,the title compound was characterized by IR and 1HNMR.CONCL |
| Key words: isatoic anhydride phthalimide synthesis |
