| 引用本文: | 阮昊1，林斌2，周方2，陈碧莲1，祝明1.CGC测定五灵止痛胶囊中冰片的含量[J].中国现代应用药学,2009,(4):326-328. |
| RUAN Hao1, LIN Bin2, ZHOU Fang2, CHEN Bilian1,ZHU Ming1.Determination of Borneolum Syntheticum in Wulingzhitong Capsules by CGC[J].Chin J Mod Appl Pharm(中国现代应用药学),2009,(4):326-328. |
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| 摘要: |
| 目的 建立测定五灵止痛胶囊中冰片的含量。方法 采用毛细管气相色谱法测定，色谱柱为INNOWAX毛细管色谱柱，FID检测器；程序升温，初始80 ℃，每分钟5 ℃升至150 ℃。结果 冰片浓度在0.100～10.015 mg·mL-1内线性关系良好（r=1.000），平均回收率为98.8%（RSD＝1.0％）。结论 CGC法操作简便、快速、准确，可有效控制五灵止痛胶囊的质量。 |
| 关键词: 毛细管气相色谱法 五灵止痛胶囊 冰片 |
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| Determination of Borneolum Syntheticum in Wulingzhitong Capsules by CGC |
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RUAN Hao1, LIN Bin2, ZHOU Fang2, CHEN Bilian1,ZHU Ming1
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| Abstract: |
| OBJECTIVE To establish a method for the determination of borneolum syntheticum in Wulingzhitong capsules. METHODS The analysis was carried out on an INNOWAX capillary column and FID detector.The initial column temperature was 80 ℃ and then raised (5 ℃·min-1) to 150 ℃. RESULTS The linear range was 0.100-10.015 mg·mL-1（r＝1.000）for borneolum syntheticum.The average recovery was 98.8 %（RSD=1.0%）.
CONCLUSION This CGC method is simple, quick, accurate and available for quality control of Wulingzhitong capsules. |
| Key words: CGC Wulingzhitong capsules borneolum syntheticum |
