引用本文: | 苗宇1;杨庆敏2;李学庆2;张晓友2;李炳阳2.牛磺酸镁盐制备工艺的改进[J].中国现代应用药学,2006,(3):205-206. |
| MIAO Yu~(1),YANG Qing-min~(2),LI Xue-qing~(2),ZHANG Xiao-you~(2),LI Bing-yang~(2).Improved synthetic process of magnesium taurate salt[J].Chin J Mod Appl Pharm(中国现代应用药学),2006,(3):205-206. |
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摘要: |
目的研究牛磺酸镁盐的制备工艺,以提高产物收率。方法以酸碱中和反应合成牛磺酸镁盐,采用正交试验对制备工艺进行优选。结果改进后最佳工艺条件:反应温度80℃;反应时间5h;牛磺酸与氢氧化镁投料摩尔比2∶1(氢氧化镁略过量)。结论该工艺合理,操作简便,收率可达55%。 |
关键词: 牛磺酸镁盐 制备工艺 正交试验 |
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Improved synthetic process of magnesium taurate salt |
MIAO Yu~(1),YANG Qing-min~(2),LI Xue-qing~(2),ZHANG Xiao-you~(2),LI Bing-yang~(2)
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Abstract: |
OBJECTIVE To study the synthetic process of magnesium taurate salt for improving the production's yield.METHODS Magnesium taurate salt(MTS) was synthesized with the method of acid-alkali neutralizing reaction,and the optimum conditions of the synthesis pr |
Key words: magnesium taurate salt synthetic process orthogonal experiment |